Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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ISO is the most rigorous in terms of defining test methods, and says which alloys should use which test methods as follows:.
All austenitic stainless steels should meet this requirement, if proper annealing took place. R Adtm, Corrosion Tests and Standards: As 15 hours is a difficult test period in practice, and is astj a minimum, conducting the test for 20 hours overnight means that the two tests are equivalent. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.
ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.
To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur. Just remember that these tests were devised for specific groups of alloys and should not be applied to all CRAs! SEP method 3 is a special environment only suitable for the Ni-Mo alloys, as described below, in section 4.
The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. ASTM G28 does not require samples to be heat treated.
Intergranular corrosion is the proper use, though the specification calls it attack, corrosion is what is taking place. Vickers Hardness 5Kg and 10Kg. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.
For an alloy that is not z262, look for an alloy with a similar composition to a listed astk to determine the most suitable test. The effect of post weld surface treatments on the corrosion resistance of super duplex stainless steel welds in sea water The samples are weighed at each interval to axtm mass loss and degree of susceptibility to intergranular attack.
This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility. Contact us a2662 for pricing or a quote! ISO is the most rigorous in terms of defining test methods, and says which alloys should use which test methods as follows: Choosing the correct method s rely on a complete understanding of your material and processes, as well as the a622 of corrosion itself.
When a test has been selected, follow the detailed directions in that standard for making up the test solution, the preparation of test samples and the finish to be used. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use.
ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.
How do you select the right ASTM corrosion testing method for your material? This test should be avoided for most CRAs, except in the circumstances described below, in section 4.
ASTM G28 method B is a more aggressive test than method A and is intended for more corrosion resistant alloys, as listed in the document. Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.
Intergranular Corrosion Testing: An Overview of ASTM A262
The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test. The etch structure types used to classify the specimens are: Asfm 1 below shows the various methods for four common standards: Where no specific test is specified, Table 5 suggests the most appropriate alongside a second choice, if the first is declined.
There is several cause for SCC, Chloride is the leading cause of transgranular cracking or attack.
G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.
This specification is for detecting susceptibility to intergranular attack IGA. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance. If you are not sure, please contact us for assistance.